Chemical products for industrial use — General method for determination of traces of sulphur compoun...
Describes a method based on prior conversion of the sulphur compounds in a test portion to sulphate, if required, and reduction of the sulphate ions ti hydrogen sulphide by a mixture of hydriodic and phosphinic acids in the presence of hydrochloric acid. The hydrogen sulphide is entrained in a current of nitrogen and absorbed in a solution of sodium hydroxide in aqueous acetone, followed by…
Boric acid, boric oxide, disodium tetraborates and crude sodium borates for industrial use — Determi...
Specifies a method applicable to products in which the nickel content being determined exceeds 0,1 mg/kg. The principle of determination is based on dissolution of a test portion, formation of the coloured nickel furil -dioxime complex, extraction with chloroform and photometric measurement at a wavelength of about 435 nm.
Crude sodium borates for industrial use — Determination of alkali-soluble copper and manganese conte...
Describes a method applicable to products in which the alkalisoluble copper and manganese contents excess 0,25 and 0,5 mg/kg, respectively. The principle consists in successively determining the manganese and copper contents of the two coloured complexes obtained during the analysis, followed by photometric measurements at wavelengths of about 435 nm and 450 nm, respectively.
Crude sodium borates for industrial use — Determination of carbonate content — Gravimetric method
Covers a method based on reaction of the carbonate in a test portion with hydrochloric acid, absorption of the released carbon dioxide in soda asbestos and measurement of the increase in mass.
Sodium perborates for industrial use — Determination of degree of attrition
Specifies a method, the principle of which consists in breaking down a sample by a high velocity jet of air in a small fluidized bed, calculating the amount of breakdown (attrition) from the change in particle size distribution of the test portion before and after fluidization, and expressing the degree of attrition as the increase in the percentage of material which passes through a screen of…