This method is applicable to the zinc alloys defined in ISO 301. It is suitable for the determination of magnesium contents between 0,01 and 0,08 %. ISO 3750 specifies principle, reagents, apparatus, sampling, procedure, expression of results and test report.
Cryolite, natural and artificial — Determination of fluorine content — Modified Willard-Winter metho...
Specifies the determination for natural and synthetic materials having a molar ratio sodium fluoride/aluminium trifluoride between 3 and 1,7 approximately. The principle consists in fusion of a test portion with sodium carbonate, separation of fluorine by distillation with sulphuric acid or perchloric acid. Titration with thorium nitrate solution in presence of sodium alizarinsulphonate/methylene…
Cryolite, natural and artificial — Determination of iron content — 1,10- Phenanthroline photometric ...
Applies for the determination of natural and synthetic materials having a molar ratio sodium fluoride/aluminium trifluoride between 3 and 1,7 approximately. The method is applicable to products having an iron content equal to or greater than 0,020 % (m/m). The principle consists in dissolution of a test portion by either alkaline or acid fusion. Reduction of iron(III) with hydroxylammonium…
Aluminium oxide primarily used for the production of aluminium — Determination of silica content — R...
The method is applicable to products having a silica content between 0.005 % (m/m) and 0.025 % (m/m) provided that the content of phosphorus pentoxide plus vanadium pentoxide does not exceed 0.02 % (m/m). The principle of the method is based on the formation of oxidized molybdosilicate (yellow) under well-defined conditions of acidity, concentration of reagents, temperature and time. Selective…
Sulphur for industrial use — Determination of arsenic content — Silver diethyldithiocarbamate photom...
Applicable to products having As contents equal or more than 0.5 mg/kg. In a well-ventilated cupboard, dissolution of a test portion in carbon tetrachloride. Oxidation of sulphur by bromine and nitric acid. Heating in a boiling water bath to eliminate the exess of bromine, carbon tetrachloride and nitric acid. The analysis is carried out according to ISO 2590. The replacement of some reagents…
Wrought steels — Macroscopic methods for assessing the content of non-metallic inclusions
Macroscopic methods deal with non-metallic inclusions visible to the naked eye or with the aid of a magnifying glass with a magnification of not more than X 10. Only inclusions equal to or greater than 1 mm long are taken into consideration. Covers the blue fracture test method, the step machined test method, the magnetic particle inspection method.
Essential oils — Estimation of primary and secondary free alcohols content by acetylation in pyridin...
The method consists in acetylating the hydroxyl groups containing compounds with a mixture of acetic anhydride and pyridine. The excess of acetic anhydride is hydrolized and the acetic acid formed is titrated with a potassium hydroxide solution. Primary and secondary alcoholes are acetylated completely by this method. Phenols, anthranilates and aldehydes are acetylated either completely or…
Phosphoric acid and sodium phosphates for industrial use (including foodstuffs) — Determination of f...
Applicable to products the F content of which is equal to or more than 0.5 mg/kg. Specifies the separation of the element from a test portion by steam distillation in a phosphoric acid medium. Formation of a blue-coloured complex with a combined reagent alizarin complexone/lanthanum nitrate in a buffered medium at the pH of 4.6. Addition of acetone to increase the stability of the complex and the…
