Aluminium oxide primarily used for the production of aluminium — Preparation and storage of test sam...
Specifies the preparation of laboratory samples, crude samples for the determination of certain geometric properties and physical and pysico-chemical tests including the determination of moisture content and dried samples. The principle consists in grinding and sieving of the sample until passing completely through a sieve of meshes having apertures of 0,2 mm. Mixing and drying at about 300 °C.…
Aluminium oxide primarily used for the production of aluminium — Determination of iron content — 1,1...
Applicable to Fe contents, expressed as Fe2 O3 , equal to or more than 0.005 % (m/m). Specifies the preliminary reduction of iron (III) by means of hydroxylammonium chloride. Formation of the iron(II)-1,10-phenanthroline complex in a buffered (pH value between 3.5 and 4.2). Photometric measurement at a wavelength of about 510 nm. Replaces ISO Recommendation R 805/1968.
Aluminium oxide primarily used for the production of aluminium — Determination of manganese content ...
Applicable to products having a Mn content between 0.0002 % (m/m) and 0.005 % (m/m). Preliminary extraction by the method specified in the annex if the apparatus available does not have a sufficient sensitivity. Describes the dissolution of a test sample by heating in a sealed borosilicate glass tube with hydrochloric acid at a controlled temperature of 250 °C. Aspiration of the solution in an…
Cryolite, natural and artificial — Determination of calcium content — Flame atomic absorption method
Describes the preparation of the calibration graph and the dissolution of a test portion in concentrated sulphuric acid and heating on a hot-plate until the hydrofluoric acid has evaporated. Treatment of the residue with concentrated hydrochloric acid. Aspiration of the solution into an acetylene/dinitrogen monoxide flame and spectrophotometric measurement of the absorption of the 422.7-nm line…
Cryolite, natural and artificial, and aluminium fluoride for industrial use — Determination of water...
Applies to the simultaneous determination of the loss of mass at 550 °C which is the sum of the masses of water that has not undergone any reaction and of the hydrogen fluoride formed by pyrohydrolysis and the mass of water released at 550 °C determined by the Karl-Fischer Method (direct electrometric titration). Makes reference to ISO 760. The difference between these two determinations is due…
This method is applicable to the zinc alloys defined in ISO 301. It is suitable for the determination of magnesium contents between 0,01 and 0,08 %. ISO 3750 specifies principle, reagents, apparatus, sampling, procedure, expression of results and test report.
Cryolite, natural and artificial — Determination of fluorine content — Modified Willard-Winter metho...
Specifies the determination for natural and synthetic materials having a molar ratio sodium fluoride/aluminium trifluoride between 3 and 1,7 approximately. The principle consists in fusion of a test portion with sodium carbonate, separation of fluorine by distillation with sulphuric acid or perchloric acid. Titration with thorium nitrate solution in presence of sodium alizarinsulphonate/methylene…
Cryolite, natural and artificial — Determination of iron content — 1,10- Phenanthroline photometric ...
Applies for the determination of natural and synthetic materials having a molar ratio sodium fluoride/aluminium trifluoride between 3 and 1,7 approximately. The method is applicable to products having an iron content equal to or greater than 0,020 % (m/m). The principle consists in dissolution of a test portion by either alkaline or acid fusion. Reduction of iron(III) with hydroxylammonium…
