Ethanol for industrial use — Methods of test — Part 9: Determination of esters content — Titrimetric...
The method is applicable to products having esters contents in the range 0.005 % (m/m) to 0.15 % (m/m). The principle consists in the saponification of esters present in a test portion by boiling with excess standard volumetric sodium hydroxide solution; determination of the residual sodium hydroxide, and hence the amount used for saponification, by titration with standard volumetric hydrochloric…
Ethanol for industrial use — Methods of test — Part 3: Estimation of content of carbonyl compounds p...
The method is applicable to products having carbonyl compounds contents between 0.00025 % (m/m) and 0.01 % (m/m). The principle is based on reaction in acid medium of the carbonyl compounds in a test portion with 2,4-dinitrophenylhydrazine. Formation of the corresponding 2,4-dinitrophenylhydrazones which, after making the solution alkaline, take on a red coloration. Photometric measurement of…
Ethanol for industrial use — Methods of test — Part 4: Estimation of content of carbonyl compounds p...
The method is applicable to products having carbonyl compounds contents equal to or greater than 0.01 % (m/m). The method only allows determination of those carbonyl compounds which react under the specified conditions. The principle is based on the reaction of hydroxylammonium chloride with the carbonyl compounds in a test portion and titration of the hydrochloric acid formed with standard…
Ethanol for industrial use — Methods of test — Part 5: Determination of aldehydes content — Visual c...
The method is applicable to products having aldehyde contents in the range 0.00025 % (m/m) to 0.00125 % (m/m). The principle is based on the reaction of the aldehydes present in a test portion with Schiff reagent. Visual comparison of the colour obtained with the colours of standard colorimetric solutions containing known quantities of acetaldehyde. - International Standards ISO 1388/1 to ISO…
Carbonaceous materials for the production of aluminium — Pitch for electrodes — Determination of con...
Specifies a conventional gravimetric method for the determination. A test portion ist reated with quinoline in a beaker at 70 to 80 °C for 15 to 20 min. Then the dissolved test portion and the residue are brought to a Hartley funnel fitted with a filter pad, and are filtered. The washed and dried residue on the filter pad is weighed.
General method for determination of silicon content — Reduced molybdosilicate spectrophotometric met...
Specifies a method based on the depolymerization of any polymerized silica by treatment with sodium fluoride in the presence of hydrochloride acid resulting in the formation of the oxidized molycdosilicate, followed by the selective reduction of this complex in the presence of oxalic acid and in a sulphuric acid medium, and spectrophotometric measurement of the blue-coloured complex at the…
Ethanol for industrial use — Methods of test — Part 7: Determination of methanol content (methanol c...
The principle is based on the conversion of methanol present in a test portion to formaldehyde by oxidation. The oxidation is carried out with a solution of potassium permanganate in phosphoric acid. Reaction of the formaldehyde formed with chromotropic acid (4,5-dihydroxynaphthalene-2,7-disulphonic acid). Photometric measurement of the violet coloration obtained at a wavelength of about 570 nm…
Ethanol for industrial use — Methods of test — Part 8: Determination of methanol content (methanol c...
The principle is based on the conversion of the methanol present in a test portion to formaldehyde by oxidation with a solution of potassium permanganate in phosphoric acid. Reaction of the formaldehyde formed with Schiff reagent. Visual comparison of the colour obtained with the colours of standard colorimetric solutions containing known quantities of formaldehyde. - International Standards ISO…
Ethanol for industrial use — Methods of test — Part 10: Estimation of hydrocarbons content — Distill...
The principle is based on distillation of a test portion in the presence of water, addition to the distillate of a saturated sodium chloride solution and measurement of the volume of insoluble hydrocarbons. A Hempel fractionating column with Liebig condenser is used for the distillation. - International Standards ISO 1388/1 to ISO 1377/12 cancel and replace ISO Recommendation R 1388-1970 of which…
Ethanol for industrial use — Methods of test — Part 1: General
The document also specifies the methods to be used for the determination of density at 20 °C, for the determination of dry residue after evaporation on a water bath, for the determination of water content, and for the measurement of colour. - International Standards ISO 1388/1 to 1388/12 cancel and replace ISO Recommendation R 1388-1970 of which they constitute a technical revision.
