Photography — Photographic-grade chemicals — Test methods — Part 6: Determination of halide content
The method is based on weighing the test portion, dissolution in water, transfer of a 20 ml aliquot in a beaker, pipetting halide standard A or B into a second beaker, adding nitric acid solution plus silver nitrate solution to each beaker, dilution with water, transfer of the treated solutions into separate Nessler colour-comparison cylinders, and observing the turbidity of the two solutions.
Photography — Photographic-grade chemicals — Test methods — Part 10: Determination of sulfide conten...
The method is based on weighing a test portion, dissolution in water, transfer to one of the Nessler colour-comparison cylinders, pipetting the volume of sulfide standard into the second Nessler colour-comparison cylinder, addition of alkaline lead solution, making up with water, mixing thoroughly, and comparing the colour and clarity of the two solutions.
Acid-grade and ceramic-grade fluorspar — Determination of manganese content — Periodate spectrometri...
Applicable to products having Mn-contents in the range 0,006 % to 0,4 %. Decomposition of the test portion with nitric and perchloric acids. After dilution follows oxidation of manganese to permanganate with sodium metaperiodate. Spectrometric measurement at 545 nm.
Animal and vegetable fats and oils — Determination of residual technical hexane content
The method is based on desorption of volatile hydrocarbons by heating at 80 °C in a closed vessel after addition of an internal standard and determination of the particular volatile hydrocarbons content of the headspace by gas chromatography using packed or capillary columns.
Iron ores — Determination of calcium content — Flame atomic absorption spectrometric method
The method is based on decomposition of the test portion by hydrochloric acid/nitric acid, evaporation, ignition of the residue and removal of silica, fusion with sodium carbonate and dissolution of the cooled melt in the filtrate, aspiration of the solution into the flame of an atomic absorption spectrometer, and comparison of the absorbance values obtained for calcium with those obtained from…
Iron ores — Determination of magnesium content — Flame atomic absorption spectrometric method
The method is based on decomposition of the test portion by hydrochloric acid/nitric acid, evaporation, ignition of the residue and removal of silica, fusion with sodium carbonate and dissolution of the cooled melt in the filtrate, aspiration of the solution into the flame of an atomic absorption spectrometer, and comparison of the absorbance values obtained for magnesium with those obtained from…
Iron ores — Determination of aluminium content — Part 1: Flame atomic absorption spectrometric metho...
The method is based on decomposition of the test portion by hydrochloric acid/nitric acid, evaporation, ignition of the residue and removal of silica, fusion with sodium carbonate and dissolution of the cooled melt in the filtrate, aspiration of the solution into the flame of an atomic absorption spectrometer, and comparison of the absorbance values obtained for aluminium with those obtained from…
Iron ores — Determination of silicon content — Part 1: Gravimetric methods
The method is based on decomposition of the test portion by 1) sintering with sodium peroxide and treatment with hydrochloric and perchloric acids and treatment with dilute nitric acid, or 2) treatment with hydrochloric, nitric and perchloric acids, evaporation, filtration of silica with any residue, fusion with sodium carbonate and dissolution in hydrochloric and perchloric acids, in both cases…
Iron ores — Determination of silicon content — Part 2: Reduced molybdosilicate spectrophotometric me...
The method is based on decomposition of the test portion by fusion with sodium tetraborate and treatment with dilute nitric acid, addition of ammonium molybdate to convert silicate into a molybdatosilicate complex, reduction to molybdenum blue with ascorbic acid, and spectrophotometric measurement of the absorbance of the molybdenum blue complex at a wavelength of approximately 600 nm. Applies to…
Direct reduced iron — Determination of carbon and/or sulfur content — High frequency combustion meth...
The method is based on combustion of the test portion in a refractory crucible in a flow of oxygen in the presence of an accelerator, conversion of the carbon present into carbon dioxide and the sulfur present into sulfur dioxide, and measurement of each gas by infrared absorption. Applies to carbon contents between 0,05 % and 2,5 % and/or sulfur contents between 0,001 % and 0,05 % in direct…
