Methods of Testing Pulp and Paper Kappa Number of Pulp
This National Standard of Canada is based on International Standard ISO
302:1981.
1.1 The Kappa number test is used for evaluation of pulps with regard to the
degree of delignification and bleachability.
1.2 The method can be applied to pulps produced in yields up to about 65% and
giving Kappa numbers not higher than 100 on hardwood pulps, and not higher than
120 on softwood pulps (Note 1).…
Oils of sassafras and nutmeg — Determination of safrole and cis- and trans-isosafrole content — Gas ...
A small quantity of the oils is analyzed by gas chromatography under specified conditions on a packed column. The safrole and cis- and trans-isosafrole contents are determined by using the internal standard method. As stationary phase are used polydimethylsiloxane, or polyethylene glycol 20000. Operating temperatures: Oven: isotherm about 100 °C when using polydimethylsiloxane; isotherm about 125…
Oils of thujone-containing Artemisia and oil of sage (Salvia officinalis Linnaeus) — Determination o...
A small quantity of the oils is analyzed under specified conditions. The alpha- and beta-thujone contents are determined by using the internal standard or addition method. As stationary phase are used cyanopropyl methylphenyl methyl silicone, or trifluoropropylmethyl silicone, or polyethylene glycol 1500. Operating temperatures: Oven: isotherm about 100 °C when using cyanopropyl methylphenyl…
Oil of calamus — Determination of cis-beta-asarone content — Gas chromatographic method on packed co...
A small quantity of the oil is analyzed under specified conditions. The cis-beta-asarone contents is determined by using the internal standard or addition method. As stationary phase polyethylene glycol 20000 is used. Operating temperatures: Oven: isotherm about 190 °C. Injection system and detector: about 170 °C.
Oils of lemon and petitgrain citronnier, and oil of lime obtained by a mechanical process — Determin...
The method consists in analyzing a small quantity of essential oil on a column of small diameter but great length under specified conditions. The citral content is determined by using the internal standard method. Polyethylene glycol 20000 is used as stationary phase. Operating temperatures: Oven: linear temperature programming from 80 to 180 °C at a rate of 2 °C/min. Injection system: about 190…
Oil of rosewood — Determination of alpha-terpineol content — Gas chromatographic method on packed co...
A small quantity of the oil is analyzed by gas chromatography under specified conditions on a packed column. The
alpha
-terpineol content is determined by using the internal standard method. Operating temperatures: Oven: isotherm between 120 and 150 °C. Injection system: about 170 °C. Detector: about 170 °C.
Ethanol for industrial use — Methods of test — Part 3: Estimation of content of carbonyl compounds p...
The method is applicable to products having carbonyl compounds contents between 0.00025 % (m/m) and 0.01 % (m/m). The principle is based on reaction in acid medium of the carbonyl compounds in a test portion with 2,4-dinitrophenylhydrazine. Formation of the corresponding 2,4-dinitrophenylhydrazones which, after making the solution alkaline, take on a red coloration. Photometric measurement of…
Ethanol for industrial use — Methods of test — Part 7: Determination of methanol content (methanol c...
The principle is based on the conversion of methanol present in a test portion to formaldehyde by oxidation. The oxidation is carried out with a solution of potassium permanganate in phosphoric acid. Reaction of the formaldehyde formed with chromotropic acid (4,5-dihydroxynaphthalene-2,7-disulphonic acid). Photometric measurement of the violet coloration obtained at a wavelength of about 570 nm…